Xceptional Instruments

Specialty & Fine Chemicals

Specialty Chemicals

Reactive extrusion, masterbatch development, and additive compounding at micro scale — validate chemistry before committing to production tonnage.

01 / 05OVERVIEW

Specialty chemical development often involves expensive raw materials, hazardous intermediates, or proprietary formulations where waste minimization is critical. The Three-Tec micro-extrusion platform allows chemists to validate reactive extrusion parameters, develop masterbatch concentrates, and compound functional additives with as little as 1 g of material. High torque density across all barrel diameters handles viscous melts and highly filled systems (>60 wt%) without stalling. The closed barrel architecture and optional ATEX-rated configurations support processing of solvent-containing or flammable feedstocks. Every run generates a complete process log for technology transfer to production-scale equipment.

02 / 05CHALLENGES

Reactive extrusion requires precise residence-time and temperature control
Masterbatch development involves highly filled systems with extreme viscosity
Raw materials may be hazardous, expensive, or available only in small quantities
Process parameters must transfer predictably to production-scale twin-screw extruders
Solvent-containing or flammable feedstocks require ATEX-rated equipment

03 / 05WORKFLOW

How it comes together.

01

Define reaction or compounding target with process chemistry team

02

Select barrel diameter and L/D ratio based on residence-time requirements

03

Feed via gravimetric ZD 5 FB i6000 for repeatable additive dosing

04

Process on ZE-series extruder with full torque, pressure, and temperature monitoring

05

Pelletize or collect extrudate for analytical confirmation and scale-up documentation

04 / 05TEST LAB

Run it in our lab first.

Our Piscataway, NJ facility is equipped to run feasibility studies for this application. Ship your material and we’ll process it on validated equipment — onsite observation or video-call available.

Explore the Lab
Reactive extrusion feasibility studies
Masterbatch and concentrate development
High-fill compounding (>60 wt%)
Process parameter documentation for technology transfer

Talk to an engineer about your application.

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